TASK 70-33-92-300-503 Procedure To Electroplate Aluminum With Nickel

DMC:V2500-00-70-33-92-00A-653A-D|Issue No:001.00|Issue Date:2013-03-20

Export Control

EAR Export Classification: Not subject to the EAR per 15 C.F.R. Chapter 1, Part 734.3(b)(3), except for the following Service Bulletins which are currently published as EAR Export Classification 9E991: SBE70-0992, SBE72-0483, SBE72-0580, SBE72-0588, SBE72-0640, SBE73-0209, SBE80-0024 and SBE80-0025.

Copyright

© IAE International Aero Engines AG (2001, 2014 - 2021) The information contained in this document is the property of © IAE International Aero Engines AG and may not be copied or used for any purpose other than that for which it is supplied without the express written authority of © IAE International Aero Engines AG. (This does not preclude use by engine and aircraft operators for normal instructional, maintenance or overhaul purposes.).

Applicability

All

Common Information

TASK 70-33-92-300-503 Procedure To Electroplate Aluminum With Nickel

Table of Contents

Introduction

Safety Precautions

Consumable Materials

Remove Faulty Nickel Deposits from Aluminum

Prepare the Parts

Nickel Plate the Aluminum

Examine the Parts

Introduction

This procedure specifies the method to electroplate aluminum or aluminum alloy parts with nickel. Nickel electroplate is a ductile coating with high internal tensile stress.

Preliminary Requirements

Pre-Conditions

NONE

Support Equipment

NONE

Consumables, Materials and Expendables

NameManufacturerPart Number / IdentificationQuantityRemark
CoMat 01-277 KEROSINELOCALCoMat 01-277
CoMat 02-017 WAXLOCALCoMat 02-017
CoMat 02-038 MASKING WAX COMPOUND (HIGH TEMPERATURE)IE514CoMat 02-038
CoMat 05-003 ABRASIVE MEDIUM ALUMINUM OXIDE, 120/220 GRADELOCALCoMat 05-003
CoMat 02-008 PUMICE POWDERLOCALCoMat 02-008
CoMat 01-085 ETHYLENE GLYCOL (ETHANEDIOL)LOCALCoMat 01-085
CoMat 07-014 STOPPING-OFF LACQUERLOCALCoMat 07-014
CoMat 02-153 ALUMINIUM WIRELOCALCoMat 02-153
CoMat 02-154 ALUMINIUM WIREIE200CoMat 02-154
CoMat 01-076 METHYL ETHYL KETONELOCALCoMat 01-076
CoMat 02-014 TERYLENE BAGLOCALCoMat 02-014
CoMat 03-017 PLATING ANODELOCALCoMat 03-017

Spares

NONE

Safety Requirements

WARNING

THIS PROCEDURE INCLUDES THE USE OF SODIUM CYANIDE OR POTASSIUM CYANIDE. CYANIDE SALTS AND/OR SOLUTIONS ARE VERY POISONOUS AND WORK VERY QUICKLY. CYANIDE SALTS RELEASE HYDROCYANIC GAS WHEN MIXED WITH ACID. HYDROCYANIC GAS CAN KILL VERY QUICKLY.

WARNING

IT IS THE RESPONSIBILITY OF THE OPERATOR TO OBTAIN AND OBSERVE THE MANUFACTURER'S MATERIAL SAFETY DATA SHEETS FOR CONSUMABLE MATERIALS. THESE CONTAIN INFORMATION SUCH AS, HAZARDOUS INGREDIENTS, PHYSICAL/CHEMICAL CHARACTERISTICS, FIRE, EXPLOSION, REACTIVITY, HEALTH HAZARD DATA, PRECAUTIONS FOR SAFE HANDLING, USE AND CONTROL MEASURES AND ALSO TO TAKE LOCAL REGULATIONS IN TO CONSIDERATION.

WARNING

YOU MUST USE THE PROTECTIVE CLOTHING SUPPLIED, WHICH INCLUDES FULL FACE AND EYE PROTECTION, AND RUBBER GLOVES.

WARNING

ALL SOLUTION IN THE EYES MUST BE REMOVED IMMEDIATELY. CLEAN THE EYES WITH WATER, SUFFICIENT TO REMOVE THE CONTAMINATION. EYE-WASH BOTTLES MUST BE PROVIDED AS CLOSE AS POSSIBLE TO THE PLACE OF WORK. GO FOR MEDICAL AID IMMEDIATELY.

WARNING

FINGERNAILS MUST BE KEPT SHORT AND MUST ALWAYS BE FULLY CLEANED BEFORE YOU EAT, DRINK, OR SMOKE.

WARNING

THE INSTRUCTIONS GIVEN BY THE SAFETY OFFICER MUST ALWAYS BE OBEYED.

WARNING

SAFETY NOTICES MUST BE PLACED IN A CONSPICUOUS PLACE.

WARNING

CYANIDE PRECAUTIONS
CYANIDE MUST ALWAYS BE KEPT AT A SAFE LOCATION, WHERE ACCESS IS ONLY AVAILABLE TO APPROVED PERSONS. YOU MUST NOT EAT, DRINK, OR SMOKE AT SUCH LOCATIONS.
CYANIDE SALTS AND SOLUTIONS MUST ALWAYS BE KEPT AWAY FROM ACIDS.
A SUPPLY OF CYANIDE ANTIDOTE MUST ALWAYS BE IMMEDIATELY AVAILABLE.
ITEMS THAT ARE USED TO EAT OR DRINK WITH MUST NOT BE KEPT AT LOCATIONS WHERE CYANIDE IS KEPT OR USED.
POISONING WILL OCCUR IF YOU SWALLOW CYANIDE, IF YOU BREATHE HYDROCYANIC GAS, OR IF CYANIDE OR HYDROCYANIC GAS ABSORBS THROUGH YOUR SKIN.
WARNING INDICATIONS OF POISONING ARE; DIZZINESS, NAUSEA, GENERAL WEAKNESS, HEADACHE, PALPITATIONS, FEELING OF SUFFOCATION AND TIGHTNESS IN THE THROAT, AND/OR, PALLOR, DEEP BREATHING, AND UNCONSCIOUSNESS.

WARNING

SODIUM HYDROXIDE PRECAUTIONS
A SUPPLY OF BUFFERED PHOSPHATE SOLUTION MUST ALWAYS BE IMMEDIATELY AVAILABLE TO APPLY TO BURNS.
CAREFULLY ADD TO WATER COMPOUNDS WHICH CONTAIN SOLID SODIUM HYDROXIDE, BECAUSE HEAT IS RELEASED WHEN THE COMPOUND DISSOLVES. MAKE MUCH MOVEMENT OF THE SOLUTION, WITH AIR OR MECHANICAL METHODS, AS YOU ADD THE COMPOUND TO THE SURFACE OF THE SOLUTION. DO NOT ADD LARGE QUANTITIES OF THE COMPOUND TO ONE SMALL AREA OF THE TANK BECAUSE THE SOLUTION WILL BOIL.

WARNING

ACID PRECAUTIONS
BE VERY CAREFUL TO KEEP THE SOLUTION AWAY FROM YOUR EYES AND BARE SKIN. WEAR PROTECTIVE CLOTHING (THIS INCLUDES EYE PROTECTION AND RUBBER GLOVES) WHEN YOU PREPARE AND USE THE NITRIC ACID SOLUTION. EXAMINE RUBBER GLOVES REGULARLY FOR PIN HOLES AND REPLACE IF NECESSARY. IF CONTAMINATION OF THE EYES OR SKIN OCCURS, FLUSH YOUR SKIN WITH A LARGE QUANTITY OF CLEAN FLOWING WATER. GET MEDICAL AID IMMEDIATELY.
FOR ALL BURNS, HOWEVER SLIGHT, GO IMMEDIATELY TO THE NEAREST MEDICAL PERSONNEL OR FIRST AID POST FOR FIRST AID.
TELL THE MEDICAL PERSONNEL WHICH SOLUTION CAUSED THE BURN, PARTICULARLY IF HYDROFLUORIC ACID IS A PART OF THE MAKE-UP.
BE SURE HYDROFLUORIC ACID BURN JELLY IS AVAILABLE AS CLOSE AS POSSIBLE TO THE WORK AREA.

Procedure

    1. SUBTASK 70-33-92-330-001 Remove Faulty Nickel Deposits from Aluminum

    2. Remove oil, grease, or carbon deposits, if necessary, with CoMat 01-277 KEROSINE, or aqueous clean by the SPM TASK 70-11-03-300-503.

      NOTE

      Thick nickel deposits can be reduced in thickness to a dimension a small amount greater than the pre-plate dimension by machining before final chemical removal of the residue.
      1. Chemically remove the faulty nickel plate.

      2. Degrease the components by the SPM TASK 70-11-03-300-503 (aqueous cleaning) if necessary.

      3. Remove the nickel electroplate with nitric acid Solution Code 28, made up to the SPM TASK 70-33-27-330-501, SUBTASK 70-33-27-180-004.

      4. Examine the part to make sure all the plating was removed. Do the chemical removal step again, as necessary.

      5. Wash the parts fully in clean cold water.

      6. Remove the masks.

      7. Put the parts fully in clean hot water at 185 deg F (85 deg C) minimum.

      8. Remove the remaining water with a blast of clean dry air.

    3. Do a non-destructive inspection of the part by the method specified in the Engine Manual.

    1. SUBTASK 70-33-92-180-001 Prepare the Parts

    2. Degrease the components by the SPM TASK 70-11-03-300-503 (aqueous cleaning) if necessary.

    3. Make sure the parts are fully dry and free from all remaining cleaning solution.

    4. Dry abrasive blast the area to be plated with CoMat 05-003 ABRASIVE MEDIUM ALUMINUM OXIDE, 120/220 GRADE (refer to the SPM TASK 70-12-02-120-501). Do not use a higher pressure than necessary, or stay in one place for longer than necessary.

    5. Rub the surface to be plated with CoMat 02-008 PUMICE POWDER on a clean, soft, grease-free wet cloth.

    6. Wash the parts in clean cold water to remove all remaining material.

      1. Mask the part with wax.

        NOTE

        Do not let the CoMat 01-085 ETHYLENE GLYCOL (ETHANEDIOL) or CoMat 07-014 STOPPING-OFF LACQUER touch other surfaces of the part because this will stop adhesion of the wax to the surface.
      2. Apply CoMat 01-085 ETHYLENE GLYCOL (ETHANEDIOL), or CoMat 07-014 STOPPING-OFF LACQUER, to the surfaces that must not be coated with wax to prevent adhesion of the wax mask.

      3. Put the parts into a bath of CoMat 02-017 WAX at the temperature specified by the manufacturer (typically 194 deg F (90 deg C) approx.). Let the parts increase in temperature to that of the bath and then remove the parts. This will produce a thin initial layer with good adhesion.

      4. Do the wax dip two more times to produce a wax coating approximately 0.0625 inch (1.57 mm) thick.

    7. While the wax is still warm, cut carefully around the edges and peel off the excess wax to expose the surface to be plated. The edges of the wax must stay adherent to prevent spread of the plating solution onto surfaces not to be plated.

    8. Remove the CoMat 01-085 ETHYLENE GLYCOL (ETHANEDIOL), or CoMat 07-014 STOPPING-OFF LACQUER with CoMat 01-277 KEROSINE. Rub the surface to be plated with CoMat 02-008 PUMICE POWDER on a soft cloth made wet with water to remove surface residue.

    9. Wash the part fully in cold flowing water.

    1. SUBTASK 70-33-92-330-002 Nickel Plate the Aluminum

    2. Put the parts to be plated onto a suitable plating fixture, or wire the parts for suspension in the cleaning and plating tanks with CoMat 02-153 ALUMINIUM WIRE, or CoMat 02-154 ALUMINIUM WIRE, or of suitable diameter applicable to the plating current.

    3. Make sure the electrical contacts are correctly placed.

    4. Aqueous degrease the parts and fixture by the SPM TASK 70-11-03-300-503.

    5. WARNING

      DO NOT LET THE ACID MIXTURE TOUCH YOUR SKIN OR EYES. WEAR PROTECTIVE EQUIPMENT.

      Etch the parts in a solution of nitric acid-hydrofluoric acid. Put the parts fully in the solution kept at 59 to 77 deg F (15 to 25 deg C) for approximately two minutes. Refer to the SPM TASK 70-33-08-100-501, SUBTASK 70-33-08-100-003 for the make up of the nitric acid-hydrofluoric acid mixture.

    6. Flush the components in cold water to remove all remaining acid.

    7. CAUTION

      DO NOT LET PARTS STAY IN THE ZINCATE SOLUTION LONGER THAN NECESSARY BECAUSE DAMAGE TO THE SURFACE OF THE PARTS CAN OCCUR.

      Put the parts fully in the zincate solution for the time specified by the manufacturer. For guidance, this is typically between for one to two minutes at 59 to 77 deg F (15 to 25 deg C). Refer to the SPM TASK 70-33-08-100-501, SUBTASK 70-33-08-100-004 for the make-up of the zincate solution.

    8. Flush the components in cold water to remove all remaining solution.

    9. Put the parts fully in the nitric acid to remove smut for between one and two minutes at 59 to 77 deg F (15 to 25 deg C). Refer to the SPM TASK 70-33-08-100-501, SUBTASK 70-33-08-100-005 for the make-up of the nitric acid solution.

    10. Flush the components in cold water to remove remaining nitric acid.

    11. CAUTION

      DO NOT LET PARTS STAY THE ZINCATE SOLUTION LONGER THAN NECESSARY BECAUSE DAMAGE TO THE SURFACE OF THE PARTS CAN OCCUR.

      Put the parts fully in the zincate solution again to apply the second zincate coating. Refer to manufacturer's instructions for the immersion time, which typically is 30 to 60 seconds at ambient temperature.

      NOTE

      For aluminum castings, if necessary, do the nitric acid etch, cold water flush and immersion in the zincate solution again. Then flush fully with water.
    12. Flush the parts in cold water to remove remaining zincate.

      1. Deposit a base (strike) layer of one of these methods:

      2. Copper Electroplate.

      3. WARNING

        THIS STEP USES A CYANIDE SOLUTION.

        Put the parts fully into the copper electroplating solution made up to the SPM TASK 70-33-92-100-501, SUBTASK 70-33-92-180-003.

      4. Keep the parts in the solution for 5 minutes at a current density of 2 amps/sq dm (20 amps/sq ft) or a voltage of 0.5 to 1.5 volts.

        1. Electroless Nickel.

          Use this step if the it is not permitted to use the Copper cyanide solution.

        2. Put the parts fully into the electroless nickel solution made up to the SPM TASK 70-33-08-100-501.

        3. Keep the parts in the solution for 10 minutes.

    13. Flush the parts fully in cold flowing water to remove all remaining unwanted material.

    14. With the current switched on, put the parts fully into one of the nickel electroplating solutions made up to the instructions in the SPM TASK 70-33-92-100-501. Keep the parts in the solution for the time necessary to get the specified plating thickness. For recommended plating parameters, refer to the solution manufacturer.

    15. Remove the parts from the plating solution and flush fully in clean cold water.

      1. Remove the stop-off as follows:

      2. To remove CoMat 02-017 WAX stop-off, put the parts fully in clean boiling water.

    16. Dry the parts with a blast of clean, dry air.

    17. If necessary, apply a corrosion preventive. Refer to the SPM TASK 70-38-05-380-501, SUBTASK 70-38-05-380-001.

    1. SUBTASK 70-33-92-220-001 Examine the Parts

    2. If necessary, remove corrosion preventive with CoMat 01-277 KEROSINE.

    3. Do a visual inspection of the parts to make sure that the nickel plate is smooth, adherent, and free from burns and blisters.

    4. Make sure the specified thickness of deposit is sufficient.

    5. Apply a corrosion preventive to the parts. Refer to the SPM TASK 70-38-05-380-501, SUBTASK 70-38-05-380-001.

Requirements After Job Completion

Follow-On Conditions

NONE
Manufacturer Code:IE200
Enterprise Name:DELETED, REFER TO CAGE CODE 00BB6
Manufacturer Code:IE514
Enterprise Name:DELETED. Was SASOL WAX AMERICAS, INC.
Manufacturer Code:LOCAL
Enterprise Name:LOCALLY SUPPLIED
Manufacturer Code:LOCAL
Supply Number:CoMat 01-076
Type:sp01
Supply Short Name:CoMat 01-076 METHYL ETHYL KETONE
Supply Name:CoMat 01-076 METHYL ETHYL KETONE
Specification Groups:
Doc NumberType
METHYL ETHYL KETONE, TECHNICAL GRADE, CERTIFIED TO BSI BS 1940 OR ASTM D740, OR TT-M-261
Suppliers:
ManufacturerRemarks
LOCAL
Manufacturer Code:LOCAL
Supply Number:CoMat 01-085
Type:sp01
Supply Short Name:CoMat 01-085 ETHYLENE GLYCOL (ETHANEDIOL)
Supply Name:CoMat 01-085 ETHYLENE GLYCOL (ETHANEDIOL)
Specification Groups:
Doc NumberType
OMAT: 107 (RR REF)COMMERCIAL GRADE B.S.2537:1955 MIL-A-46153
JCR-166COMMERCIAL GRADE B.S.2537:1955 MIL-A-46153
Suppliers:
ManufacturerRemarks
LOCAL
k3504
IE200
K6835
70657
Manufacturer Code:LOCAL
Supply Number:CoMat 01-277
Type:sp01
Supply Short Name:CoMat 01-277 KEROSINE
Supply Name:CoMat 01-277 KEROSINE
Specification Groups:
Doc NumberType
OMAT: 101COMMERCIAL GRADE D.ENG.RD2494 MIL-T-5624 TYPE JP5
Suppliers:
ManufacturerRemarks
LOCAL
IE108
Manufacturer Code:41753
Supply Number:CoMat 02-008
Type:sp01
Supply Short Name:CoMat 02-008 PUMICE POWDER
Supply Name:CoMat 02-008 PUMICE POWDER
Specification Groups:
Doc NumberType
JCR-117200 GRADE
SS-P-821GDFFF PMC 3001200 GRADE
OMAT: 201200 GRADE
Suppliers:
ManufacturerRemarks
41753
LOCAL
K6835
V557V
Manufacturer Code:LOCAL
Supply Number:CoMat 02-014
Type:sp01
Supply Short Name:CoMat 02-014 TERYLENE BAG
Supply Name:CoMat 02-014 TERYLENE BAG
Specification Groups:
Doc NumberType
OMAT: 2/51TERYLENE OR POLYPROPYLENE BAG
Suppliers:
ManufacturerRemarks
LOCAL
K6835
IE446
Manufacturer Code:LOCAL
Supply Number:CoMat 02-017
Type:sp01
Supply Short Name:CoMat02-017 WAX
Supply Name:CoMat 02-017 WAX
Specification Groups:
Doc NumberType
11429Y/Y MIL-P-23242 OMAT: 228PLATING WAX WILKINS CAMPBELL
JCR-178PLATING WAX WILKINS CAMPBELL
Suppliers:
ManufacturerRemarks
LOCAL
K6835
K4404
Manufacturer Code:X111X
Supply Number:CoMat 02-038
Type:sp01
Supply Short Name:CoMat 02-038 MASKING WAX COMPOUND (HIGH TEMPERATURE)
Supply Name:CoMat 02-038 MASKING WAX COMPOUND (HIGH TEMPERATURE)
Specification Groups:
Doc NumberType
DELETED
Suppliers:
ManufacturerRemarks
X111X
Manufacturer Code:LOCAL
Supply Number:CoMat 02-153
Type:sp01
Supply Short Name:CoMat 02-153 ALUMINIUM WIRE
Supply Name:CoMat 02-153 ALUMINIUM WIRE
Specification Groups:
Doc NumberType
OMAT: 21818 S.W.G. 0.048 IN DIA
JCR-17618 S.W.G. 0.048 IN DIA
Suppliers:
ManufacturerRemarks
LOCAL
IE200
K6835
Manufacturer Code:IE200
Supply Number:CoMat 02-154
Type:sp01
Supply Short Name:CoMat 02-154 ALUMINIUM WIRE
Supply Name:CoMat 02-154 ALUMINIUM WIRE
Specification Groups:
Doc NumberType
OMAT: 21916 S.W.G 0.064IN DIA
JCR-17716 S.W.G 0.064IN DIA
Suppliers:
ManufacturerRemarks
IE200
Manufacturer Code:LOCAL
Supply Number:CoMat 03-017
Type:sp01
Supply Short Name:CoMat 03-017 PLATING ANODE
Supply Name:CoMat 03-017 PLATING ANODE
Specification Groups:
Doc NumberType
OMAT:2/56NICKEL, DURVANIC OR DEPOLARIZED 99.00 - 100.00 % PURITY
Suppliers:
ManufacturerRemarks
LOCAL
IE366
IE233
IE234
IE322
K6835
Manufacturer Code:X222X
Supply Number:CoMat 05-003
Type:sp01
Supply Short Name:CoMat 05-003 ABRASIVE MEDIUM ALUMINUM OXIDE, 120/220 GRADE
Supply Name:CoMat 05-003 ABRASIVE MEDIUM ALUMINUM OXIDE, 120/220 GRADE
Specification Groups:
Doc NumberType
Use one of the CoMat 05-003 letter suffix alternatives.
Suppliers:
ManufacturerRemarks
X222X
Manufacturer Code:LOCAL
Supply Number:CoMat 07-014
Type:sp01
Supply Short Name:CoMat 07-014 STOPPING-OFF LACQUER
Supply Name:CoMat 07-014 STOPPING-OFF LACQUER
Specification Groups:
Doc NumberType
OMAT:7/40DFORTELAC
Suppliers:
ManufacturerRemarks
LOCAL
IE366
K6835